Oxidation effects on spark plasma sintering of molybdenum nanopowders

Full densification of Molybdenum powders using Spark Plasma Sintering

Pure molybdenum powder was sintered using Spark Plasma Sintering under various temperatures, and holding times, under a pressure of 77 MPa and a heating rate at 700°C/min. After sintering, a carbide layer was observed at the surface. The carbide layer thickness, the relative density of the sample as well as the microhardness and the grain size of Mo were measured. The carbide thickness depends ...

Spark plasma sintering of alumina nanopowders produced by electrical explosion of wires

Alumina nanopowders produced by electrical explosion of wires were sintered using the spark plasma sintering technique. The results of XRD analysis show that the main phase in the compacted nanopowders is α-Al2O3. According to the SEM observations, the sintered alumina nanopowder consists of micron-sized faceted grains and nano-sized necked grains. The increase in sintering temperature resulted...

Spark Plasma Sintering of Negative Temperature Coefficient Thermistor Ceramics

Application of Spark Plasma Sintering for Manufacturing of Thermoelectric Materials

V-VI thermoelectric compounds like Bi2Te3-based alloys are well known for room temperature applications like Peltier coolers or thermogenerators. Their anisotropic physical properties and mechanical weakness are a problem for the manufacturing. To overcome the mechanical problem Spark Plasma Sintering (SPS) was used. 2 inch Wafers of polycrystalline bismuth telluride based n-type and p-type the...

Spark plasma sintering of ductile ceramic particles: study of LiF

Densification of cuboidal micrometer-sized lithium fluoride particles as ductile ceramic by spark plasma sintering (SPS) was investigated. Specimens were fabricated at different pressures and temperature conditions, ranging from 2 to 100 MPa at 500 C and from 200 to 700 C under 100 MPa of applied pressure, respectively. Dense specimens of 99 % relative density were fabricated by heating to 500 ...